학회 | 한국화학공학회 |
학술대회 | 2005년 가을 (10/21 ~ 10/22, 인하대학교) |
권호 | 11권 2호, p.2509 |
발표분야 | 재료 |
제목 | Synthesis of LiFePO4 powder as a cathode material for Li-ion batteries by spray pyrolysis |
초록 | LiFePO4 particles as a cathode material for lithium ion batteries were prepared by the conventional spray pyrolysis. Because they were very sensitive to the reductive atmosphere, H2 5%/Ar 95% mixed gas was used as a carrier gas for both spray pyrolysis and post treatment. The reaction temperature was varied between 400 to 800℃ and prepared particles were post treated at 750℃ for 4 hours with the flow rate of 0.4 L/min to get LiFePO4 single phase. The morphology and crystallinity of the prepared particles were characterized by scanning electron microscope (SEM) and X-ray diffraction analysis. Doped lithium iron phosphate was prepared to improve their intrinsic low conductivity by the same method above and its conductivity at room temperature was characterized by 4-point probe method. |
저자 | 조문영, 박승빈 |
소속 | 한국과학기술원 |
키워드 | Lithium ion batteries; cathode material; lithium iron phosphate; conductivity |
원문파일 | 초록 보기 |