Thin Solid Films, Vol.516, No.22, 8117-8124, 2008
X-ray diffraction peak profile analysis aiming at better understanding of the deformation process and deformed structure of a martensitic steel
Microstructural characteristics of extra low carbon lath martensite after cold rolling to 85% reduction and equal-channel angular pressing of four passes were studied by means of X-ray diffraction (XRD) peak profile analysis and transmission electron microscopy. The modified Willilamson-Hall and Warren-Averbach methodologies were implemented to determine crystallite size distribution, distribution density and character of prevailing dislocations of the deformed structures. Cold-rolled steel showed lamellar dislocation boundaries which subsequently disappear at large strain by equal-channel angular pressing, turning to a highly and uniformly dislocated structure involving equiaxed ultrafine grains. XRD peak profile analysis revealed that upon further straining of lath martensite; i) crystallite size decreases, ii) dislocation density increases slightly and iii) fraction of screw dislocations increases. (C) 2008 Elsevier B.V. All rights reserved.
Keywords:Maraging steel;Ultrafine grain;Lath martensite;Equal-channel angular pressing;X-ray diffraction peak profile