화학공학소재연구정보센터
Journal of Industrial and Engineering Chemistry, Vol.19, No.1, 322-326, January, 2013
Novel cyclic sulfonium iodide containing siloxane high performance electrolyte for dye-sensitized solar cell
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A new type of solid and gel state electrolytes based on siloxane cyclic sulfonium iodides was synthesized and used in dye-sensitized solar cells. The resulting electrolytes were characterized by 1H NMR, TGA, diffusion coefficient, and ion conductivity. The thermo-oxidative stabilities of the prepared ionic species are lower than that of DMII because the bond strength of S+-C in thiophenium is lower than that of N+-C in imidazolium. Among the three SiCSIs based electrolytes, SiCSI3 showed a maximum photoconversion efficiency of 7.3%. In addition, the performance of the DSSCs showed relatively reasonable compared with the imidazolium type DMII electrolyte.
  1. Hurley FH, Wier TP, Journal of the Electrochemical Society., 98, 203 (1951)
  2. Wilkes JS, Zaworotko MJ, Journal of the Chemical Society, Chemical Communications., 965 (1992)
  3. Gratzel M, Journal of Photochemistry and Photobiology C., 4, 145 (2003)
  4. Hagfeldt A, Gratzel M, Accounts of Chemical Research., 33, 269 (2000)
  5. Wu J, Lan Z, Lin J, Huang M, Hao S, Sato T, Yin S, Advanced Materials., 19, 4006 (2006)
  6. Stathatos E, Lianos P, Lavrencic-Stangar U, Orel B, Adv. Mater., 14(5), 354 (2002)
  7. Hao S, Wu J, Huang Y, Lin J, Solar Energy., 80, 209 (2006)
  8. Agrell HG, Lindgren J, Hagfeldt A, Solar Energy., 75, 169 (2003)
  9. Jin HM, Seo DW, Lee SH, Lim YD, Islam MM, Kim WG, J. Ind. Eng. Chem., 18(4), 1499 (2012)
  10. Bai Y, Cao Y, Zhang J, Wang M, Li R, Wang P, Shaik MZ, Gratzel M, Nature Materials., 7, 626 (2008)
  11. Nishida T, Tashiro Y, Yamamoto M, Journal of Fluorine Chemistry., 120, 135 (2003)
  12. Suarez PA, Selbach VM, Dullius JE, Einloft S, Piatnicki CM, Azambuja DS, Desouza RF, Dupont J, Electrochim. Acta, 42(16), 2533 (1997)
  13. McFarlane DR, Sun J, Golding J, Meakin P, Forsyth M, Electrochim. Acta, 45(8-9), 1271 (2000)
  14. Bonhote P, Dias AP, Papageorgiou N, Kalyanasundaram K, Gratzel M, Inorg. Chem., 35(5), 1168 (1996)
  15. Huddleston JG, Visser AE, Reichert WM, Willauer HD, Broker GA, Robin DR, Green Chemistry., 3, 156 (2001)
  16. Tokuda H, Hayamizu K, Ishii K, Abu Bin Hasan Susan M, Watanabe M, J. Phys. Chem. B, 108(42), 16593 (2004)
  17. Seo DW, Parvez MK, Lee SH, Kim JH, Kim SR, Lim YD, Kim WG, Electrochimica Acta., 57, 285 (2011)
  18. Seo DW, Sarker S, Nath NCD, Choi SW, Ahammad AJS, Lee JJ, Kim WG, Electrochim. Acta, 55(4), 1483 (2010)
  19. MacFarlane DR, Meakin P, Sun J, Amini N, Forsyth M, J. Phys. Chem. B, 103(20), 4164 (1999)
  20. Zhou ZB, Matsumoto H, Tatsumi K, Chemistry: A European Journal., 11, 752 (2005)
  21. Seo DW, Lim YD, Lee SH, Ur SC, Kim WG, Bulletin of the Korean Chemical Society., 32, 8 (2011)
  22. Sesto RED, Corley C, Robertson A, Wilkes JS, Journal of Organometallic Chemistry., 690, 2536 (2005)
  23. Stegemann H, Rhode A, Reiche A, Schnittke A, Fuellbier H, Electrochimica Acta., 37, 379 (1992)
  24. Yang L, Zhang ZX, Gao XH, Zhang HQ, Mashita K, J. Power Sources, 162(1), 614 (2006)
  25. Fang S, Yang L, Wei C, Peng C, Tachibana K, Kamijima K, Electrochemistry Communications., 9, 2696 (2007)
  26. Okoturo OO, VanderNoot TJ, J. Electroanal. Chem., 568(1-2), 167 (2004)
  27. Guo L, Pan X, Wang M, Zhang C, Fang X, Chen S, Dai S, Solar Energy., 85, 7 (2011)
  28. Lee SH, Konkuk University, Novel siloxane bisimidazolium diiodide as high performance electrolytes for DSSC, MS Thesis (2011)
  29. Brook MA, Silicon in Organic, Organometallic and Polymer Chemistry, John Wiley & Sons, New York, Ch 9, 256. (2000)
  30. Hauch A, Georg A, Electrochim. Acta, 46(22), 3457 (2001)
  31. Lestel L, Cheradame H, Boileau S, Polymer., 31, 1154 (1990)