Silan based paraoxon memories onto QCM electrodes

Ebru Birlik Ozkutuk; Sibel Emir Diltemiz; Elif Ozalp; Arzu Ersoz; Rıdvan Say

Journal of Industrial and Engineering Chemistry, Vol.19, No.6, 1788-1792, November, 2013

DOI10.1016/j.jiec.2013.02.021 Export Citation

Silan based paraoxon memories onto QCM electrodes

Ebru Birlik Ozkutuk^†, Sibel Emir Diltemiz¹, Elif Ozalp, Arzu Ersoz¹, and Rıdvan Say¹

Department of Chemistry, Eskisehir Osmangazi University, Eskisehir, Turkey
¹Department of Chemistry Anadolu University, Eskisehir, Turkey

E-mail:

In this study, a novel quartz crystal microbalance (QCM) based on the modification of paraoxon- imprinted polymer onto a QCM with a high selectivity and sensitivity has been developed for the determination of paraoxon. The QCM sensor has characterized using AFM and ellipsometer. The performance of the QCM sensor has evaluated and presented good reproducibility, shorter response time (20 min), wider linear range (0.02-10 μM) and low detection limit (0.02 μM). The results have shown that the selectivity of QCM sensor has found as being very high in the presence of parathion which is similar in structure with paraoxon.

Keywords:QCM;Paraoxon;Sensor;MIP

[References]

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Cano MLC, Vidal JLM, Gonzalez FJE, Galera MM, Journal of Chromatographic Science., 39, 345 (2001)
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Ye L, Mosbach K, Chemistry of Materials., 20, 859 (2008)
Ozkutuk EB, Ersoz A, Denizli A, Say R, J. Hazard. Mater., 157(1), 130 (2008)
Alexander C, Andersson HS, Andersson LI, Ansell RJ, Kirsch N, Nicholls IA, O’Mahony J, Whitcombe MJ, Journal of Molecular Recognition., 19, 106 (2006)
Birlik E, Erso¨ z A, Denizli A, Say R, Analytica Chimica Acta., 565(2), 145 (2006)
Pizzariello A, Stred’ansky M, Stred’anska S, Miertus S, Sensors and Actuators B: Chemical., 76, 286 (2001)
Hirayama K, Sakai Y, Kameoka K, Noda K, Naganawa R, Sensors and Actuators B:Chemical., 86, 20 (2002)
Ersoz A, Diltemiz SE, Ozcan AA, Denizli A, Say R, Sensors and Actuators B: Chemical., 137, 7 (2009)
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Birlik Ozkutuk E, Emir Diltemiz S, Ozalp E, Say R, Ersoz A, Materials Science and Engineering: C., 33, 938 (2013)
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[1] Mulchandani A, Chen W, Mulchandani P, Wang J, Rogers KR, Biosensors & Bioelectronics., 16, 225 (2001)

[2] Khaled E, Hassana HNA, Mohamedb GG, Ragabc FA, Aly Eldin A, Seleimc, Talanta., 83, 357 (2010)

[3] Cano MLC, Vidal JLM, Gonzalez FJE, Galera MM, Journal of Chromatographic Science., 39, 345 (2001)

[4] Karim KNS, Das BC, Khalequzzaman M, Pakistan Journal of Zoology., 33(2), 105 (2001)

[5] Jeannot R, Sauvard E, Analusis., 27, 271 (1999)

[6] Wiskur SL, Ait-Haddou H, Lavigne JJ, Anslyn EV, Accounts of Chemical Research., 34, 963 (2001)

[7] Epstein JR, Walt DR, Chemical Society Reviews., 32, 203 (2003)

[8] Rakow NA, Suslick KS, Nature., 406, 710 (2000)

[9] Ye L, Mosbach K, Chemistry of Materials., 20, 859 (2008)

[10] Ozkutuk EB, Ersoz A, Denizli A, Say R, J. Hazard. Mater., 157(1), 130 (2008)

[11] Alexander C, Andersson HS, Andersson LI, Ansell RJ, Kirsch N, Nicholls IA, O’Mahony J, Whitcombe MJ, Journal of Molecular Recognition., 19, 106 (2006)

[12] Birlik E, Erso¨ z A, Denizli A, Say R, Analytica Chimica Acta., 565(2), 145 (2006)

[13] Pizzariello A, Stred’ansky M, Stred’anska S, Miertus S, Sensors and Actuators B: Chemical., 76, 286 (2001)

[14] Hirayama K, Sakai Y, Kameoka K, Noda K, Naganawa R, Sensors and Actuators B:Chemical., 86, 20 (2002)

[15] Ersoz A, Diltemiz SE, Ozcan AA, Denizli A, Say R, Sensors and Actuators B: Chemical., 137, 7 (2009)

[16] Sener G, Ozgur E, Yılmaz E, Uzun L, Say R, Denizli A, Biosensors and Bioelectronics., 26, 815 (2010)

[17] Say R, Gultekin A, Atılır Ozcan A, Denizli A, Ersoz A, Analytica Chimica Acta., 640, 82 (2009)

[18] Marx KA, Biomacromolecules, 4(5), 1099 (2003)

[19] Hao RZ, Song HB, Zuo GM, Yang RF, Wei HP, Wang DB, Cui ZQ, Zhang ZP, Cheng ZX, Zhang XE, Biosensors and Bioelectronics., 26, 3398 (2011)

[20] Wang R, Li Y, Biosensors and Bioelectronics., 42, 148 (2013)

[21] Alves CA, Pedroso MM, de Moraes MC, Souza DHF, Cass QB, Faria RC, Biochem. Biophys. Res. Commun., 408(4), 571 (2011)

[22] Yan M, Wang D, Xie J, Liu C, Cheng J, Chow CWK, Leeuwen J, Journal of Hazardous Materials., 215-216, 115 (2012)

[23] Percival CJ, Stanley S, Braithwaite A, Newton MI, McHale G, Analyst (Cambridge, UK)., 127, 1024 (2002)

[24] Dickert FL, Lieberzeit P, Tortschanoff M, Sensors and Actuators B: Chemical., 65, 186 (2000)

[25] Windeln J, Bram C, Eckes HL, Hammel D, Huth J, Marien J, Rohl H, Schug C, Wahl M, Wienss A, Applied Surface Science., 179(1), 168 (2001)

[26] Wyszynski B, Somboon P, Nakamoto T, Sensors and Actuators B: Chemical., 121(2), 538 (2007)

[27] Nishiyama K, Takakusagi Y, Kusayanagi T, Matsumoto Y, Habu S, Kuramochi K, Sugawara K, Sakaguchi K, Takahashi H, Natsugari H, Kobayashi S, Bioorganic and Medicinal Chemistry., 17(1), 195 (2009)

[28] Percival CJ, Stanley S, Galle M, Braithwaite A, Newton MI, McHale G, Hayes W, Analytical Chemistry., 73, 2001 (4225)

[29] Sauerbrey G, Zeitschrift fur Physik A., 155, 206 (1959)

[30] Marx S, Zaltsman A, International Journal of Environmental Analytical Chemistry, 83, 671 (2003)

[31] Say R, Analytica Chimica Acta., 579, 74 (2006)

[32] Birlik Ozkutuk E, Emir Diltemiz S, Ozalp E, Say R, Ersoz A, Materials Science and Engineering: C., 33, 938 (2013)

[33] Malitesta C, Losito I, Zambonin PG, Analytical Chemistry., 71, 1366 (1999)

[34] Yan S, Gao Z, Fang Y, Cheng Y, Zhou H, Wang H, Dyes Pigments., 74, 572 (2007)

[35] Zhang T, Liu F, Chen W, Wang J, Li K, Analytica Chimica Acta., 450, 53 (2001)

[36] Alizadeh T, Thin Solid Films, 518(21), 6099 (2010)