Journal of Food Engineering, Vol.117, No.4, 521-529, 2013
Characterization of co-crystallized sucrose entrapped with cardamom oleoresin
Cardamom oleoresin emulsified with gum acacia was encapsulated by co-crystallization in a supersaturated sucrose solution to prepare flavoured sucrose cubes. The co-crystals with and without cardamom oleoresin were characterized at 25 degrees C and 33%, 63% and 93% relative humidity for hygroscopicity and crystallinity vis-a-vis pure crystal sucrose. Co-crystallized sucrose cubes showed lower hygroscopicity at 93% relative humidity, a longer dissolution time, and a decreased crystallinity as compared to crystal sucrose. The active components of cardamom oleoresin such as 1,8-cineole (30.23%) and alpha-terpinyl acetate (46.42%) in cardamom oleoresin was quantified by gas chromatography. The encapsulation efficiency of 1,8-cineole and alpha-terpinyl acetate in lab-made co-crystallized sucrose cubes was approximately 35.23% and 67.18%, respectively. This approach could contribute to value addition of cardamom oleoresin for flavoured tea and also have potential applications in traditional Indian sweets. (C) 2012 Elsevier Ltd. All rights reserved.
Keywords:Co-crystallization;Cardamom oleoresin;Gum acacia;Sucrose;Encapsulation;Hygroscopicity and crystallinity