화학공학소재연구정보센터
Materials Science Forum, Vol.416-4, 335-340, 2003
The energy balance during plasma sintering
High heating rate during plasma sintering of metallic powders, mainly the supersolidus, can lead to better properties of the sintered material. In this work, powders with different thermal conductivities (Cu and Ni) were plasma sintered using both, planar discharge and hollow cathode discharge (HCD) configuration. The thermal evolution was studied using three thermocouples inserted inside the samples at different depths. Thermal gradient and the heating rate were measured as a function of the source power; discharge configuration, pressure and thermal conductivity of the material. We have observed that the thermal gradient changed greatly with the discharge configuration. The thermal difference between most profound and most shallow inserted thermocouple in Cu samples was around 30 degreesC for both planar and HCD discharge configuration. Ni samples and the planar configuration gave thermal difference of 70 degreesC while for HCD configuration thermal difference went superior 140 degreesC. For this last case, heating rate of 300 degreesC/min was obtained.