Journal of Industrial and Engineering Chemistry, Vol.20, No.5, 3709-3713, September, 2014
Hydrothermal synthesis of CuS nanostructures and their application on preparation of ABS-based nanocomposite
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Copper sulfide nanoparticles were synthesized via a novel hydrothermal reaction between
Cu(NO3)·24H2O and thioglycolic acid. Thioglycolic acid is used as sulfur source and capping agent simultaneously. CuS nanoparticles were then added to acrylonitrile-butadiene-styrene (ABS) copolymer. The thermal stability behavior of ABS filled with copper sulfide nanoparticles was investigated by thermogravimetric analysis (TGA). Nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy and atomic force microscopy (AFM). The flame retardancy behavior of ABS-CuS was studied by UL-94 analysis.
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