Journal of Industrial and Engineering Chemistry, Vol.21, 884-888, January, 2015
Synthesis and characterization of ZnO nanohemispheres via solution-phase thermal decomposition and its comparison with the solid-phase approach
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ZnO nanohemispheres are successfully synthesized via thermal decomposition approach using [bis(2-hydroxy-1-naphthaldehydato)zinc(II)] complex, as precursor. The final ZnO nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy, and photoluminescence (PL) spectroscopy. Furthermore, the same solid phase thermal treatment is preformed and the morphology is compared with the obtained ZnO nanohemispheres.
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