Synthesis and characterization of CeO2 nanoparticles via hydrothermal route

Mokhtar Panahi-Kalamuei; Sakineh Alizadeh; Mehdi Mousavi-Kamazani; Masoud Salavati-Niasari

Journal of Industrial and Engineering Chemistry, Vol.21, 1301-1305, January, 2015

DOI10.1016/j.jiec.2014.05.046 Export Citation

Synthesis and characterization of CeO2 nanoparticles via hydrothermal route

Mokhtar Panahi-Kalamuei, Sakineh Alizadeh, Mehdi Mousavi-Kamazani¹, and Masoud Salavati-Niasari^†

Institute of Nano Science and Nano Technology, University of Kashan, P.O. Box 87317-51167, Kashan, Iran
¹Young Researchers and Elites Club, Kashan Branch, Islamic Azad University, Kashan, Iran

E-mail:

Cerium oxide (CeO2) nanoparticles have been synthesized from (NH4)2Ce(NO3)6, ethylenediamine and hydrazine by a hydrothermal method. Ethylenediamine and hydrazine with pH management can control the particle growth and have an important role in the formation of nanoparticles. Various experimental parameters were examined, such as the reaction temperature, the reaction time, and the molar ratios of the starting reagents. The as-synthesized products were characterized by powder X-ray diffraction (XRD), transmission electronmicroscopy (TEM), scanning electronmicroscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), and energy dispersive X-ray spectroscopy (EDX).

Keywords:Cerium oxide (CeO2);Nanoparticles;Hydrothermal;Rare earth

[References]

Chen Y, Glumac N, Kear BH, Skandan G, Nanostruct. Mater., 9, 101 (1997)
Mousavi-Kamazani M, Salavati-Niasari M, Emadi H, Micro Nano Lett., 7, 896 (2012)
Mousavi-Kamazani M, Salavati-Niasari M, Emadi H, Mater. Res. Bull., 47(12), 3983 (2012)
Mousavi-Kamazani M, Salavati-Niasari M, Compos. Part B: Eng., 56, 490 (2014)
Mir N, Salavati-Niasari M, Sol. Energy, 86(11), 3397 (2012)
Bera P, Gayen A, Hegde MS, Lalla NP, Spadaro L, Frusteri F, Arena F, J. Phys. Chem. B, 107(25), 6122 (2003)
Jacobs G, Williams L, Graham U, Sparks D, Davis BH, J. Phys. Chem. B, 107(38), 10398 (2003)
Li RX, Yabe S, Yamashita M, Momose S, Yoshida S, Yin S, Solid State Ion., 151, 235 (2003)
Sohlberg K, Pantelides ST, Pennycook SJ, J. Am. Chem. Soc., 123(27), 6609 (2001)
Jasinski P, Suzuki T, Anderson HU, Sens. Actuators B-Chem., 95, 73 (2003)
Goubin F, Rocquefelte X, Whangbo MH, Montardi Y, Brec R, Jobic S, Chem. Mater., 16, 662 (2004)
Shchukin DG, Caruso RA, Chem. Mater., 16, 2287 (2004)
Trovarelli A, Catal. Rev.-Sci. Eng., 38(4), 439 (1996)
Colussi S, de Leitenburg C, Dolcetti G, Trovarelli A, J. Alloy. Compd., 374, 387 (2004)
Masui T, Ozaki T, Machida K, Adachi G, J. Alloy. Compd., 303-304, 49 (2000)
Trovarelli A, Boaro M, Rocchini E, de Leitenburg C, Dolcetti G, J. Alloy. Compd., 323-324, 584 (2001)
Zhou YC, Rahaman MN, J. Mater. Res., 8, 1680 (1993)
Li YX, Chen WF, Zhou XZ, Mater. Lett., 59, 48 (2005)
Yu JC, Zhang LZ, Lin J, J. Colloid Interface Sci., 260(1), 240 (2003)
Chen W, Li F, Yu J, Mater. Lett., 60, 57 (2006)
Alifanti M, Baps B, Blangenois N, Chem. Mater., 15, 395 (2003)
Zhou XD, Huebner W, Anderson HU, Chem. Mater., 15, 378 (2003)
Lee JS, Choi SC, Mater. Lett., 59, 395 (2005)
Dos Santos ML, Lima RC, Riccardi CS, Tranquilin RL, Bueno PR, Varela JA, Longo E, Mater. Lett., 62, 4509 (2008)

[Referenced By]

[1] Chen Y, Glumac N, Kear BH, Skandan G, Nanostruct. Mater., 9, 101 (1997)

[2] Mousavi-Kamazani M, Salavati-Niasari M, Emadi H, Micro Nano Lett., 7, 896 (2012)

[3] Mousavi-Kamazani M, Salavati-Niasari M, Emadi H, Mater. Res. Bull., 47(12), 3983 (2012)

[4] Mousavi-Kamazani M, Salavati-Niasari M, Compos. Part B: Eng., 56, 490 (2014)

[5] Mir N, Salavati-Niasari M, Sol. Energy, 86(11), 3397 (2012)

[6] Bera P, Gayen A, Hegde MS, Lalla NP, Spadaro L, Frusteri F, Arena F, J. Phys. Chem. B, 107(25), 6122 (2003)

[7] Jacobs G, Williams L, Graham U, Sparks D, Davis BH, J. Phys. Chem. B, 107(38), 10398 (2003)

[8] Li RX, Yabe S, Yamashita M, Momose S, Yoshida S, Yin S, Solid State Ion., 151, 235 (2003)

[9] Sohlberg K, Pantelides ST, Pennycook SJ, J. Am. Chem. Soc., 123(27), 6609 (2001)

[10] Jasinski P, Suzuki T, Anderson HU, Sens. Actuators B-Chem., 95, 73 (2003)

[11] Goubin F, Rocquefelte X, Whangbo MH, Montardi Y, Brec R, Jobic S, Chem. Mater., 16, 662 (2004)

[12] Shchukin DG, Caruso RA, Chem. Mater., 16, 2287 (2004)

[13] Trovarelli A, Catal. Rev.-Sci. Eng., 38(4), 439 (1996)

[14] Colussi S, de Leitenburg C, Dolcetti G, Trovarelli A, J. Alloy. Compd., 374, 387 (2004)

[15] Masui T, Ozaki T, Machida K, Adachi G, J. Alloy. Compd., 303-304, 49 (2000)

[16] Trovarelli A, Boaro M, Rocchini E, de Leitenburg C, Dolcetti G, J. Alloy. Compd., 323-324, 584 (2001)

[17] Zhou YC, Rahaman MN, J. Mater. Res., 8, 1680 (1993)

[18] Li YX, Chen WF, Zhou XZ, Mater. Lett., 59, 48 (2005)

[19] Yu JC, Zhang LZ, Lin J, J. Colloid Interface Sci., 260(1), 240 (2003)

[20] Chen W, Li F, Yu J, Mater. Lett., 60, 57 (2006)

[21] Alifanti M, Baps B, Blangenois N, Chem. Mater., 15, 395 (2003)

[22] Zhou XD, Huebner W, Anderson HU, Chem. Mater., 15, 378 (2003)

[23] Lee JS, Choi SC, Mater. Lett., 59, 395 (2005)

[24] Dos Santos ML, Lima RC, Riccardi CS, Tranquilin RL, Bueno PR, Varela JA, Longo E, Mater. Lett., 62, 4509 (2008)