Korean Journal of Materials Research, Vol.11, No.10, 879-888, October, 2001
Nb 첨가 Zr 합금의 미세조직과 Creep 특성에 미치는 마지막 열처리 온도의 영향
Effect of Final Annealing Temperature on Microstructure and Creep Characteristics of Nb-containing Zirconium Alloys
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The effects of final annealing temperature on the microstructure and creep characteristics were investigated for the Zr-lNb-0.2X (X=0, Mo, Cu) and Zr-lNb- 1Sn-0.3Fe-0.1X (X=0, Mo, Cu) alloys. The microstructures were observed by using TEM/EDS, and grain size and distributions of precipitates were analyzed using a image analyzer. The creep test was performed at 400 ? C under applied stress of 150 MPa for 10 days. The β -Zr was observed at annealing temperature above 600 ? C . In the temperature above 600 ? C , the grain sizes of both alloy systems appeared to be increased with increasing the final annealing temperature. The creep strengths of Zr-1Nb-1Sn-0.3Fe-0.1X alloys were higher than those of Zr-1Nb-0.2X ones due to the effect of solid solution hardening by Sn in Zr-lNb-lSn-0.3Fe-0.1X alloy system. Also, Mo addition showed the strong effect of precipitate hardening in both alloy systems. The creep strength rapidly decreased with increasing the annealing temperature up to 600 ? C . However, a superior creep resistance was obtained in the sample that annealed to have a second phase of β -Zr. It was considered that the appearance of β -Zr would play an important role in the strengthening mechanism of creep deformation.
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