Journal of Materials Science, Vol.29, No.19, 5183-5187, 1994
R-Curve Measurement of Silicon-Nitride Ceramics Using Single-Edge Notched Beam Specimens
R-curve behaviour of three kinds of silicon nitride-based ceramics has been studied using the single-edge notched beam (SENB) technique. If the notch is deep enough, the specimen shows stable fracture during the bending test, even when the sample is a brittle material. The conditions required to obtain stable fracture in the bending test are clarified by the analysis. The crack length of the specimen was also calculated from the changing load during the fracture test. In this study, coarse-grained silicon nitride shows a large increase of the R-curve. On the other hand, silicon nitride with silicon carbide whiskers shows no R-curve increase. The rise of the R-curve should be related to the microstructure of the ceramics, and especially to the grain size of the specimen, because silicon carbide whiskers are not large compared to the silicon nitride grains, and silicon carbide can reduce the grain growth of silicon nitride during sintering.