Journal of Materials Science, Vol.30, No.17, 4215-4225, 1995
Microstructure and Mechanical Characteristics of Alpha-Alumina-Based Fibers
The high-temperature mechanical behaviour of alumina-based ceramic fibres has been investigated by the comparison of a dense pure alumina fibre, a porous pure alumina fibre and a zirconia-reinforced dense fibre. Tensile and creep tests have been conducted up to 1300 degrees C in air in parallel with microstructural investigations on the as-received and tested fibres. Room-temperature behaviour of the fibres is close to that of bulk materials having the same microstructure, but the fibre form allows higher failure stresses to be attained. High-temperature deformation of the three fibres is achieved by grain-boundary sliding (epsilon proportional to sigma(2)), and is accompanied by isotropic grain growth. The specific microstructures of each fibre induce differences in the creep threshold levels as a function of temperature and stress and also in creep rates and resistance to damage. Despite better resistance to creep and damage of the zirconia-reinforced fibre, alumina-based fibres are limited to applications below 1100 degrees C. Grain boundaries are the principal cause of mechanical degradation at high temperature with these fibres.
Keywords:TRANSMISSION ELECTRON-MICROSCOPY;CONTROLLED DIFFUSIONAL CREEP;FINE-GRAINED ALUMINA;SUPERPLASTIC DEFORMATION;CERAMICS;FLOW;FRACTURE;FIBERS