Molecular Crystals and Liquid Crystals, Vol.515, 179-189, 2009
Crystal and Molecular Structure Analysis of 1-Acryloyl-3-methyl-2,6-bis(3,4,5-trimethoxyphenyl)piperidine-4-one
The title compound C27H33NO8 crystallizes in the orthorhombic crystal class under the space group Pbca with cell parameters a=13.775(4) angstrom, b=16.389(2) angstrom, c=23.085(6) angstrom, Z=8, and V=5212.6(3) angstrom 3. The piperidine ring in the structure adopts a twist boat conformation. The bond lengths and bond angles are in good agreement with the standard values. The structure exhibits intermolecular hydrogen bond of the type C-H center dot center dot center dot O. The synthesized molecule was characterized by FT-IR, 1H-NMR, MS, and elemental analysis.