The title compound, (2-((6-chloropyridin-3-yl)methoxy)-5-methylphenyl)(p-tolyl) methanone, was synthesized and characterized spectroscopically and finally confirmed by (XRD) study. The title compound crystallizes in the monoclinic space group P21/c with cell parameters a=9.4420(1)angstrom, b=7.9810(6)angstrom, c=23.777(4)angstrom, =90 degrees, =90.883(3)degrees, =90 degrees, V=1791.5(4)angstrom-3, and Z=4. The structure exhibits intermolecular hydrogen bond of the type C-H center dot center dot center dot O.