The lignan content of Linum olympicum Boiss. was investigated by HPLG and GC-M,IS in comparison with standards, and 2 phenylpropanoid glycosides, syringin (1) and coniferin (2), were isolated from the aerial parts. Identification of the 2 compounds was achieved b 7 comparison with standards using TLC and HPLC and the structures of the isolated compounds were established by UV and H-1-NMR analysis.