The coupling of a wastewater treatment anaerobic reactor with a microfiltration or ultrafiltration membrane is particularly attractive : lower sludge production than in an aerobic reactor, methane production and dissociation of the mean residence times of the different phases. However, the industrial development of such a process is hampered by the membrane fouling which can be a result of many causes and require a comprehensive study especially the fouling by anaerobic suspensions, In order to simplify the study, the different phases of the anaerobic oxidation were separated and this work is focused on the filtration of an anaerobic suspension fed with acetic acid as the sole carbon source at 2 g/l TOC. The effluent quality was excellent without sludge production in spite of large variation of the liquid phase space time. The tested filtration elements were tubular Carbosep membranes. The M14 membrane showed the greatest flux of 120 l/m(2) h at 0.5 bar and 25 Pa shear stress and the flux increased to 180 l/m(2) h when a baffle was introduced. The main fouling mechanism appears to be the particle deposition on the membrane surface as no flux decline was observed at higher cross-flow velocity.