SiAlON 원료분말제조를 위한 분무건조 과립분말의 형상과 크기에 미치는 공정변수효과

최재형; 이소율; 한윤수; 이성민; 남산; Seongwon Kim; Jae-Hyeong Choi; Soyul Lee; Yoonsoo Han; Sung-Min Lee; Sahn Nahm; 김성원

Korean Journal of Materials Research, Vol.27, No.12, 716-721, December, 2017

DOI10.3740/MRSK.2017.27.12.716 Export Citation

SiAlON 원료분말제조를 위한 분무건조 과립분말의 형상과 크기에 미치는 공정변수효과

Effect of Process Parameters on the Morphology and Size of Spray-Dried Granule Powder for Fabrication of SiAlON Raw Material

최재형^{1, 2}, 이소율¹, 한윤수¹, 이성민¹, 남산 ², Seongwon Kim^{1, †}

¹한국세라믹기술원 이천분원 엔지니어링세라믹센터
²고려대학교 신소재공학과

Jae-Hyeong Choi^{1, 2}, Soyul Lee¹, Yoonsoo Han¹, Sung-Min Lee¹, Sahn Nahm², and 김성원^{1, †}

¹Engineering Ceramics Center, Korea Institute of Ceramic Engineering & Technology, Icheon, Gyeonggi-do 17303, Republic of Korea
²Department of Materials Science and Engineering, Korea University, Anam-dong, Seongbuk-gu, Seoul 02841, Republic of Korea

E-mail:

SiAlON-based ceramics are some of the most typical ceramic materials used as cutting tools for HRSA(Heat Resistant Super-Alloys). SiAlON can be fabricated using ceramic processing, such as mixing, granulation, compaction, and sintering. Spray drying is a widely-used method for producing a granular powder of controlled morphology and size with flowability. In this study, we report a systematic investigation aimed at optimizing spherical granule morphology by controlling spray-drying parameters such as gas flow and feed rate. Before spray drying, the viscosities of the raw material slurries were also optimized with the amount of dispersant added.

Keywords:SiAlON;spray drying;granule powder;spherical morphology;spray-drying parameter

[References]

Ezugwu EO, Bonney J, Yamane Y, J. Mater. Process. Technol., 134, 233 (2003)
Ezugwu EO, Inter. J. Mach. Tools Manufact., 45, 1353 (2005)
Acikbas NC Yurdakul H, Mandal H, Kara F, Turan S, Kara A, Bitterlich B, J. European Ceram. Soc., 32, 1321 (2012)
Acikbas NC, Demir O, Ceram. Int., 39, 3249 (2013)
Schneider G, Cutting tool applications., p5-8 (2002).
Kim JW, Paik U, Yoon KJ, J. Korean Ceram. Soc., 36, 210 (1999)
Kim S, Bang SW, Hwang I, Yoon SQ, Shin H, J. Korean Ceram. Soc., 51, 324 (2014)
Wang B, Yang J, Guo R, Gao JQ, Yang JF, Mater. Charact., 60, 894 (2009)
Iijima M, Okamura N, Tatami J, Ind. Eng. Chem. Res., 54(51), 12847 (2015)
Reed JS, Principles of ceramics process, 2nd ed., p. 323-329, John wiley & Sons, Inc., USA (1995).
Shoulders WT, Bizarri G, Bourret E, Gaume RM, J. Am. Ceram. Soc., 99(1), 20 (2016)
Okuyama K, Lenggoro IW, Chem. Eng. Sci., 58(3-6), 537 (2003)
Zilberboim R, Kopelmanm I, Talmon Y, J. Food Sci., 51, 1307 (1986)
Cho YH, Shin DS, Park JY, J. Food Sci. Technol., 32, 132 (2000)
Bayvel L, Liquid Atomization, CRC Press, Taylor & Francis Group, London (1993).

[Related Articles]

[1] Ezugwu EO, Bonney J, Yamane Y, J. Mater. Process. Technol., 134, 233 (2003)

[2] Ezugwu EO, Inter. J. Mach. Tools Manufact., 45, 1353 (2005)

[3] Acikbas NC Yurdakul H, Mandal H, Kara F, Turan S, Kara A, Bitterlich B, J. European Ceram. Soc., 32, 1321 (2012)

[4] Acikbas NC, Demir O, Ceram. Int., 39, 3249 (2013)

[5] Schneider G, Cutting tool applications., p5-8 (2002).

[6] Kim JW, Paik U, Yoon KJ, J. Korean Ceram. Soc., 36, 210 (1999)

[7] Kim S, Bang SW, Hwang I, Yoon SQ, Shin H, J. Korean Ceram. Soc., 51, 324 (2014)

[8] Wang B, Yang J, Guo R, Gao JQ, Yang JF, Mater. Charact., 60, 894 (2009)

[9] Iijima M, Okamura N, Tatami J, Ind. Eng. Chem. Res., 54(51), 12847 (2015)

[10] Reed JS, Principles of ceramics process, 2nd ed., p. 323-329, John wiley & Sons, Inc., USA (1995).

[11] Shoulders WT, Bizarri G, Bourret E, Gaume RM, J. Am. Ceram. Soc., 99(1), 20 (2016)

[12] Okuyama K, Lenggoro IW, Chem. Eng. Sci., 58(3-6), 537 (2003)

[13] Zilberboim R, Kopelmanm I, Talmon Y, J. Food Sci., 51, 1307 (1986)

[14] Cho YH, Shin DS, Park JY, J. Food Sci. Technol., 32, 132 (2000)

[15] Bayvel L, Liquid Atomization, CRC Press, Taylor & Francis Group, London (1993).