Invar36 (Fe64Ni36) and Invar-Cu (Fe59Ni36Cu5) nanocrystalline compacts were successfully obtained by spark plasma sintering from mechanically alloyed powders. The coefficient of thermal expansion (CTE) was determined for both Invar36 and Invar-Cu compacts. For Invar36 powder, the lattice parameter value is constant up to 250 A degrees C, while for the Invar-Cu powder, the value of lattice parameter changes for the temperatures that exceed 160 A degrees C. Both Invar36 and Invar-Cu nanocrystalline compacts were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), and dilatometry. The value of CTE is very low for both Invar36 compact (alpha = 0.6 x 10(-6)/A degrees C) and Invar-Cu (alpha = 5.2 x 10(-6)/A degrees C) up to Curie temperature (T (C)), in agreement with in situ (high-temperature X-ray diffraction-HT-XRD) analyses of Invar-type powders.