Recovery of gold(III) from the stripping solution containing palladium (II) by ion exchange and synthesis of gold particles

Wei Dong Xing; Man Seung Lee

Journal of Industrial and Engineering Chemistry, Vol.69, 255-262, January, 2019

DOI10.1016/j.jiec.2018.09.038 Export Citation

Recovery of gold(III) from the stripping solution containing palladium (II) by ion exchange and synthesis of gold particles

Wei Dong Xing, and Man Seung Lee^†

Department of Advanced Material Science & Engineering, Institute of Rare Metal, Mokpo National University, Chonnam 534-729, Republic of Korea

E-mail:

Separation of macro amount of gold(III) from a small amount of Pd(II) was investigated by ion exchange. From the screening experiments, a nonionic resin Amberlite XAD7HP was selected for this purpose. The adsorption behavior of Au(III) onto Amberlite XAD7HP followed Langmuir isotherm. The loading capacity obtained from the isotherm agreed well with that experimentally measured. Au(III) solution with 99.99% purity was obtained by eluting the loaded Amberlite XAD7HP with the mixture of HCl and acetone. Comparative studies on the synthesis of gold particles were done from the eluate by adding ascorbic acid and K2CO3 in presence and absence of acetone.

Keywords:Gold;Palladium;Purification;Ion exchange;Gold particles

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[3] Yeh YC, Creran B, Rotello VM, Nanoscale, 4, 1871 (2012)

[4] Papasani MR, Wang G, Hill RA, Nanomed. Nanotechnol.Biol.Med., 8, 804 (2012)

[5] Cui JR, Zhang LF, J. Hazard. Mater., 158(2-3), 228 (2008)

[6] Luty-Błocho M, Wojnicki M, Fitzner K, Int. J. Chem. Kinet., 49, 789 (2017)

[7] Yang S, Ji X, Yang W, Chem. J. Chin. Univ., 37, 2125 (2016)

[8] Malassis L, Dreyfus R, Murphy RJ, Hough LA, Donnio B, Murray CB, RSC Adv., 6, 33092 (2016)

[9] Ji XH, Song XN, Li J, Bai YB, Yang WS, Peng XG, J. Am. Chem. Soc., 129(45), 13939 (2007)

[10] Kumar S, Gandhi KS, Kumar R, Ind. Eng. Chem. Res., 46(10), 3128 (2007)

[11] Zhang ZQ, Wu YH, Langmuir, 26(12), 9214 (2010)

[12] Song JY, Jang HK, Kim BS, Process Biochem., 44(10), 1133 (2009)

[13] Dwivedi AD, Gopal K, Colloids Surf. A: Physicochem. Eng. Asp., 369, 27 (2010)

[14] Snyders CA, Mpinga CN, Bradshaw SM, Akdogan G, Eksteen JJ, The Adsorption and Elution of Platinum Group Metals (Pt, Pd, and Au) from Cyanide Leach Solutions Using Activated Carbon, pp.743 2013.

[15] Wei W, Cho CW, Kim S, Song MH, Bediako JK, Yun YS, J. Mol. Liq., 216, 18 (2016)

[16] Xing W, Lee M, Senanayake G, Hydrometallurgy, 180, 58 (2018)

[17] Urbanski TS, Fornari P, Abbruzzese C, Hydrometallurgy, 55, 137 (2000)

[18] Murakami H, Nishihama S, Yoshizuka K, Hydrometallurgy, 157, 194 (2015)

[19] Yang L, Jia FF, Song SX, Sep. Purif. Technol., 186, 63 (2017)

[20] Wang F, Zhang TT, Zhang ZZ, Zhang L, Sep. Purif. Technol., 152, 108 (2015)

[21] Zhang L, Li N, Fan P, Chu X, An S, Zhang J, Wang X, Hydrometallurgy, 127-128, 8 (2012)

[22] Elshehy EA, El-Safty SA, Shenashen MA, Khairy M, Sens. Actuators B-Chem., 203, 363 (2014)

[23] Hua M, Zhang S, Pan B, Zhang W, Lv L, Zhang Q, J. Hazard. Mater., 211-212, 317 (2012)

[24] Sole KC, Mooiman MB, Hardwick E, Sep. Purif. Rev., 47, 159 (2017)

[25] Al-Merey R, Hariri Z, Hilal JA, Microchem. J., 75, 169 (2003)

[26] Fujiwara K, Ramesh A, Maki T, Hasegawa H, Ueda K, J. Hazard. Mater., 146(1-2), 39 (2007)

[27] Kim EY, Kim MS, Lee JC, Pandey BD, J. Hazard. Mater., 198, 206 (2011)

[28] Nguyen NV, Jeong J, Jha MK, Lee JC, Asare KO, Hydrometallurgy, 105, 161 (2010)

[29] Xing WD, Lee MS, Kim YH, J. Ind. Eng. Chem., 59, 328 (2018)

[30] Moawed EA, El-Shahat MF, Anal. Chim. Acta, 788, 200 (2013)

[31] Truong HT, Lee MS, Miner. Eng., 115, 13 (2018)

[32] Marczenko Z, Balcerzak M, Separation, Preconcentration and Spectropho-tometry in Inorganic Analysis, Polish Scientific Publishers PWN, Warszawa, 2000.

[33] Colombo C, Oates CJ, Monhemius AJ, Plant JA, Geochem. Explor. Environ. Anal., 8, 1 (2008)

[34] Richardson MJ, Johnston JH, Borrmann T, Eur. J. Inorg. Chem., 2006, 2618 (2006)

[35] Nguyen VT, Lee JC, Jeong J, Kim BS, Cote G, Chagnes A, Ind. Eng. Chem. Res., 54(4), 1350 (2015)

[36] Nguyen NV, Jeong J, Lee JC, J. Chem. Technol. Biotechnol., 88(6), 1014 (2013)

[37] Bernardis FL, Grant RA, Sherrington DC, React. Funct. Polym., 65(3), 205 (2005)

[38] Mironov IV, Russ. J. Inorg. Chem., 53, 655 (2008)

[39] Rajasingam R, Jayasinghe NS, Lucien FP, Tran T, Miner. Eng., 19(9), 896 (2006)

[40] Topete A, Meda MA, Alvarez EMV, Cambon A, Barbosa S, Taboada P, Mosquera V, ACS Appl. Mater. Interfaces, 6, 11142 (2014)

[41] Sun K, Qiu J, Liu J, Miao Y, J. Mater. Sci., 44, 754 (2008)

[42] Njoki PN, Lim IIS, Mott D, Park H, Khan B, Mishra S, Sujakumar R, Luo J, Zhong C, J. Phys. Chem., 111, 14661 (2007)

[43] Dong S, Yang F, Su L, Fang W, Precious Metals China, 34, 35 (2013)

[44] Marsden JO, House CL, The Chemistry of Gold Extraction, second edn., Society for Mining, Metallurgy, and Exploration, Inc., USA, 2009.

[45] Mahmoud MHH, JOM, 55, 36 (2003)

[46] Cruywagen JJ, Kriek RJ, J. Coord. Chem., 60, 439 (2007)