화학공학소재연구정보센터
Advanced Powder Technology, Vol.29, No.12, 3145-3154, 2018
Enhancing the fluidization quality of nanoparticles using external fields
Fluidization quality of beds containing alumina and iron oxide nanoparticles in the Agglomerate Bubbling Fluidization (ABF) was improved by applying a combination of vibration and magnetic field. Pressure fluctuations were measured and analyzed by Fast Fourier Transform (FFT), Recurrence Plot (RP) and Recurrence Quantitative Analysis (RQA). Results of FFT showed that the wall vibration creates a periodic signal at 100 Hz which is not originated from the bed hydrodynamics. RP of pressure fluctuations before and after applying the assisting forces showed that the white areas in the plot decrease in size, which indicates an increase in the contribution of meso-structures such as agglomerates and small bubbles. The transition in the equilibrium bed hydrodynamics, between the condition in which assisting forces are not applied and condition in which they are applied, was tracked. It was shown by the determinism of pressure fluctuations that when the iron oxide nanoparticles exist alongside with alumina nanoparticles, this transition to the new equilibrium condition was reached in a shorter time. Determinism of pressure fluctuation of beds containing iron oxide decreased after applying the assisting forces. This trend confirms that large bubbles start to disappear and become substituted by smaller structures when magnetic field is applied to the bed. Under this condition, the interphase contact efficiency increases and the bed becomes closer to the Agglomerate Particle Fluidization (APF) regime. (C) 2018 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.