화학공학소재연구정보센터
홈 로그인 로그아웃 연락처 사이트맵
Journal of Industrial and Engineering Chemistry, Vol.80, 43-52, December, 2019
DOI10.1016/j.jiec.2019.07.029  Export Citation
Microwave-assisted combustion design of magnetic Mg?Fe spinel for MgO-based nanocatalyst used in biodiesel production: Influence of heating-approach and fuel ratio
Tohid Amani1, 2, Mohammad Haghighi1, 2, †, and Behgam Rahmanivahid1, 2
  • 1Chemical Engineering Faculty, Sahand University of Technology, P.O. Box 51335-1996, Sahand New Town, Tabriz, Iran
  • 2Reactor and Catalysis Research Center (RCRC), Sahand University of Technology, P.O. Box 51335-1996, Sahand New Town, Tabriz, Iran
E-mail:
Magnetic MgO/MgFe2O4 nanocatalysts synthesized by microwave-assisted combustion method by using various fuel ratios and employed in the production of biodiesel. To evaluate the influence of microwave heating, its results were compared to those of conventional furnace. MgO was dispersed on all the samples using simple and cost-effective impregnation method. Characterizations of the magnetic spinel nanocatalysts were performed via XRD, FESEM, SPSD, BET-BJH, FTIR, TG and EDX analyses. Accordingly, the sample synthesized by microwave irradiation with a fuel ratio of 1.5 exhibited the largest effective area and pore volume and appropriate pore size for transesterification reaction with coarse molecules.
Keywords:Mg-Fe spinel;MgO-based nanocatalyst;Microwave-assisted combustion preparation;Green fuel;Heating approach
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