Activated carbon was prepared from coirpith by a chemical activation method and characterized. The adsorption of toxic heavy metals, Hg(II), Pb(II), Cd(II), Ni(II), and Cu(II) was studied using synthetic solutions and was reported elsewhere. In the present work the adsorption of toxic heavy metals from industrial wastewaters onto coirpith carbon was studied. The percent adsorption increased with increase in pH from 2 to 6 and remained constant up to 10. As coirpith is discarded as waste from coir processing industries, the resulting carbon is expected to be an economical product for the removal of toxic heavy metals from industrial wastewaters.