Butylacrylate/butylmethacrylate (BABMA) colloids were obtained by cocondensation at 17 K of the monomers with several metals such as Au, Pd, Ag, Cu, Cd, Ga, Ge, In, Sn, Sb, Bi, and Zn. The relative stability of the comonomer metal colloids at room temperature was measured. Au-, Pd-, Cd-, and Ge-BABMA colloids are the most stable. The average particle size of these clusters dispersed in the monomers ranges between 19 and 72 Angstrom. On the other hand, the metal clusters in the copolymers range from 32 to 126 Angstrom. The colloids were polymerized with 2,2'-azoisobutyronitrile and dibenzoyl peroxide using 0.1, 0.25, 0.5, and 1.0 mol % initiator at 65 degrees C to obtain poly(butylacrylate-co-butylmethacrylate) The doped copolymers yields are over 52% w/w in most of the MW fractions The viscosity average molecular weights ((M) over bar 9(v)) range between 370,000 and 970,000 g/mol for the highest MW fraction. The copolymers were characterized by means of thermogravimetry, Fourier transform IR, elemental analysis, and conductivity measurements.