Two resins were synthesized by radical polymerization using N,N'-methylene-bis-acrylamide and ammonium persulfate as the crosslinking reagent and initiator, respectively. The yields were 98%. The resins were characterized by FTIR and UV-Vis spectroscopy. Sorption behavior of resins toward Hg(II), Cd(II), Zn(II), Pb(II), and Cr(III) ions was studied at different pHs depending on the metal ion. Both resins showed selective sorption to Hg(II) ions at pH 2 from a mixture of all ions. The elution of Hg(II) bound to the resins was also investigated using perchloric acid at different concentrations.