Rheologica Acta, Vol.41, No.1-2, 134-143, 2002
Extrusion of pastes with a piston extruder for the determination of the local solid and fluid concentration, the local porosity and saturation and displacement profiles by means of NMR imaging
Nuclear Magnetic Resonance (NMR) was used to investigate the extrusion behaviour of PTFE pastes in a ram extruder. By means of H-1-NMR imaging (MRI) it is possible to determine the local proton density and therefore, the local fluid concentration. The F-19-MRI provides the local solid concentration. Thus the local saturation and the local porosity can be calculated with the information of the local fluid and solid concentration. Furthermore displacement profiles can be derived from NMR images by means of correlation techniques without any preparation or marking of the pastes.
Keywords:pastes;extrusion;piston extruder;local porosity and saturation;fluid and solid concentration;displacement profiles