The Zn-22% Al eutectoid alloy was subjected to equal-channel angular pressing at a temperature of 473 K to give an as-pressed grain size of similar to1.3 mum. Subsequent tensile testing of the as-pressed alloy at room temperature revealed a transition from deformation by a dislocation mechanism at the higher strain rates to superplastic flow at strain rates below similar to5 x 10(-3) s(-1): this corresponds to the transition from region III to region II in conventional superplasticity. Samples were pulled to relatively low total strains, of the order of similar to0.2-0.5, and the surface topography was then examined using an atomic force microscope (AFM). The AFM observations confirm the transition in deformation mechanisms with decreasing strain rate and they provide direct evidence for the occurrence of grain boundary sliding within the superplastic regime.