Powder Technology, Vol.140, No.3, 228-239, 2004
Compression of polymer bound alumina agglomerates at the micro deformation scale
In this paper, the mechanical properties of alumina particle based agglomerates, prepared in a tumble mixer by using a poly (vinyl alcohol) (PVA) binder (ca. 5% by volume) in conjunction with water solvent, are described at a micro deformation level. Uniaxial compressive deformation profiles of these alumina agglomerates, typically 180-200 mum in diameter, are reported and their diverse behaviour during compression have been observed, which vary from a clear brittle rupture to progressive ductile deformation. However, certain common patterns of the agglomerate reaction force response, as a function of the compressive displacement, are identified, such as the similarities in the reloading response after each discrete fracture event. The Hertz Theory and a slope and peak force analysis are applied to establish the common patterns and trends, and generalize the intrinsic deformation characteristics of these agglomerates. (C) 2004 Elsevier B.V. All rights reserved.
Keywords:agglomerate;mechanical behaviour;compression;micro deformation;slope analysis;peak force analysis