Chemical Engineering Science, Vol.61, No.8, 2394-2405, 2006
Investigation of fine granular material flow through a packed bed
Three different methods cut-off, time-of-flight, and Pulsed Field Gradient Nuclear Magnetic Resonance were used to study downstream flow of fine granular material through the fixed bed reactor. For describing the transport of solid particles within a fixed granular bed, a model has been developed. In time-of-flight and cut-off techniques the highest average velocity of filtration is observed at the lowest mass flow rate in all experimental traces, while upon the flow rate increase it tends to an asymptotic value. Experimental results obtained by pulsed field gradient nuclear magnetic resonance technique have revealed the bimodal character of particles velocities distribution. The average filtration velocity has a maximum at an intermediate mass flow rate close to the bed flooding, in contrast to the results obtained by cut-off and time-of-flight methods. The velocities measured using all three techniques were compared by converting them into dimensionless values. From the experimental results, the values of model parameters have been evaluated which allowed us to describe particle velocities within a bed. (c) 2005 Elsevier Ltd. All rights reserved.