Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance

Leskes M; Steuernagel S; Schneider D; Madhu PK; Vega S

Chemical Physics Letters, Vol.466, No.1-3, 95-99, 2008

DOI10.1016/j.cplett.2008.10.029 Export Citation

Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance

Leskes M, Steuernagel S, Schneider D, Madhu PK, Vega S

We report here high-resolution H-1 solid-state nuclear magnetic resonance spectra acquired by a combination of magic-angle spinning (MAS) and radiofrequency pulse methods up to MAS frequencies of 65 kHz. The details of the pulse methods and experimental conditions are outlined together with spectra from model compounds. (C) 2008 Elsevier B.V. All rights reserved.