Chemistry Letters, Vol.38, No.7, 694-695, 2009
Synthesis and Structural Characterization of a Novel Three-dimensional Molybdenum-Oxygen Framework Constructed from Mo3O9 Units
A novel three-dimensional molybdenum oxide Mo3O9 center dot H2O (1) constructed from Mo3O9 units has been successfully synthesized under hydrothermal conditions and structurally characterized by IR spectrum, inductively coupled plasma (ICP) analysis, powder X-ray diffraction (PXRD), X-ray photoelectron spectroscopy (XPS), and single-crystal X-ray diffraction.