화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2008년 봄 (04/23 ~ 04/25, 제주ICC)
권호 14권 1호, p.1274
발표분야 재료
제목 Hollow NiO nanoparticles grown by aqueous solution process
초록 Nanocrystalline, uniform-sized hollow nickel oxide (NiO) nanoparticles were synthesized in a high yield via simple solution process. The typical diameters of the hollow NiO nanoparticles were in the range of 20-30 nm as was confirmed from the FESEM and TEM observations. In a typical reaction process, initially, the Ni2+ ions were adsorbed on the negative charge carrying polystyrene nanospheres which form core-shell type nanoparticles in the solution. The further calcination of these core-shell nanoparticles would lead the formation of hollow NiO nanoparticles. The detailed structural characterizations by XRD and HRTEM confirmed the nanocrystalline nature for the as-grown NiO nanoparticles. The FTIR studies were carried to check the composition and purity of the synthesized products. Good optical properties were obtained for the as-synthesized NiO nanoparticles as was confirmed from the UV-vis spectroscopy.
저자 모하메드 바즘, Umar Ahmad, 김정현, 김진석, 한윤봉
소속 전북대
키워드 NiO; nanoparticles; solution method
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