화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2009년 봄 (04/23 ~ 04/24, 광주 김대중컨벤션센터)
권호 15권 1호, p.1025
발표분야 촉매 및 반응공학
제목 Continuous synthesis of N-doped titania particles under subcritical and supercritical water conditionsfor photocatalytic reaction under visible light
초록 In this study, N-dope titania was continuously synthesized under supercritical and subcritical water conditions using titanium(Ⅳ)tetraisopropoxide (TTIP) and nitric acid as a titania precursor and N source, respectively. The synthesized N-doped titania was characterized by XRD, SEM, N2-adsorption, XPS and UV-Visible spectroscopy. XPS results showed that N-doped titania was successfully synthesized. Accrording to the XRD patterns, the synthesized N-doped titania had pure anatase phase which is known to has higher photocatalytic activity than rutile phase. In the UV-Visible spectroscopy, the absorption edge of synthesized N-doped titania shifted into the visible light region compared with representative commercial titania P25. The photocatalytic activity of N-doped titania is discussed for the degradation of methyl orange.
저자 전주원, 김정랑, 임선기
소속 한국과학기술원
키워드 N-doped titania; supercritical hydrothermal synthesis
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