| 학회 |
한국공업화학회 |
| 학술대회 |
2012년 가을 (10/31 ~ 11/02, 대전컨벤션센터) |
| 권호 |
16권 2호 |
| 발표분야 |
포스터-정보.전자소재 |
| 제목 |
A facile route for surface functionalization of magnetic nanoparticles by polyethyleneglycol via “Thiol-Ene Click” Michale addition reaction |
| 초록 |
The magnetic nanoparticles-graft-polyethyleneglycol (MNPs-g-PEG) was synthesized via a facile “Thiol-Ene Click” Michale addition reaction. Thiol functionalized PEG (PEG-SH) was prepared by treating PEG with 3-mercaptopropionic acid to obtain PEGylated 3-mercaptopropionate. The surface of MNPs was initially functionalized by 3-methacryloxypropyltrimethoxysilane (MPTS) to introduce double bond onto MNPs surface. The MPTS anchored MNPs were reacted with PEG-SH under ultraviolet irradiation to afford covalently immobilized PEG onto MNPs. The structure, morphology, thermal, and magnetic properties of the magnetic nanocomposites were investigated by FT-IR, XPS, TEM, TGA, and SQUID analyses. |
| 저자 |
임권택, Thanh Binh Mai, Md. Rafiqul Islam, 조범활
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| 소속 |
부경대 |
| 키워드 |
magnetic nanoparticles; thiol-ene addition; click chemistry; PEGylated
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| E-Mail |
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