초록 |
3-phenoxyphthalonitrile, 4-phenoxyphthalonitrile, tetrakis(2,9,16,23-phenoxy) metal phthalocyanines and tetrakis(1,8,15,22-phenoxy) metal phthalocyanines (MPc; M = Cu, TiO, VO) were quickly synthesized through the microwave processing. In microwave processing, synthetic reaction time is much shorter with higher yield, compared to the conventional processing. All of samples were characterized by H-NMR, infrared spectroscopy (IR), UV-Vis spectroscopy (UV-Vis), X-ray diffractometry (XRD) and Maldi-Tof Mass Spectrometry (MS). |