화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2014년 봄 (04/23 ~ 04/25, 창원컨벤션센터)
권호 20권 1호, p.874
발표분야 촉매 및 반응공학
제목 Synthesis and characterization of vanadosilicates, AM-13 and AM-14
초록 Vanadium incorporated microporous material has drawn much attention because of its unique catalytic performance for partial oxidation.  In this work, two novel large-pore sodium vanadosilicates (AM-13 and AM-14) were synthesized and characterized with various spectroscopic techniques.  
For AM-13 synthesis, the amount of Ca(OH)2 affected significantly the corresponding crystalline properties while the quantity of VOSO4 was critical controling factor for the structural integrity.  Further, the structural characterization was performed using X-ray photoelectron spectroscopy.  Depending on the content of V, the oxidation state was affected, which suggested the different coordination environment around the V atom.  
저자 정하나, 조성준, 이현정, 김중현
소속 전남대
키워드 vanadosilicates
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