학회 | 한국화학공학회 |
학술대회 | 2014년 봄 (04/23 ~ 04/25, 창원컨벤션센터) |
권호 | 20권 1호, p.874 |
발표분야 | 촉매 및 반응공학 |
제목 | Synthesis and characterization of vanadosilicates, AM-13 and AM-14 |
초록 | Vanadium incorporated microporous material has drawn much attention because of its unique catalytic performance for partial oxidation. In this work, two novel large-pore sodium vanadosilicates (AM-13 and AM-14) were synthesized and characterized with various spectroscopic techniques. For AM-13 synthesis, the amount of Ca(OH)2 affected significantly the corresponding crystalline properties while the quantity of VOSO4 was critical controling factor for the structural integrity. Further, the structural characterization was performed using X-ray photoelectron spectroscopy. Depending on the content of V, the oxidation state was affected, which suggested the different coordination environment around the V atom. |
저자 | 정하나, 조성준, 이현정, 김중현 |
소속 | 전남대 |
키워드 | vanadosilicates |
원문파일 | 초록 보기 |