| 학회 |
한국고분자학회 |
| 학술대회 |
2009년 봄 (04/09 ~ 04/10, 대전컨벤션센터) |
| 권호 |
34권 1호 |
| 발표분야 |
고분자 가공/복합재료 |
| 제목 |
Preparation and characterization of nano silver colloid via non-polar solvent method. |
| 초록 |
This study is concerned with non-polar solvent method to prepare nano silver colloid. Synthesis of silver colloid has been carried out in a non-polar solvent system as toluene, in which silver nitrate served as a precursor, neodecanoic acid as capping agent and phenyl hydrazine as reductant. To confirm the size and morphology of silver nanoparticles, Silver colloid has been characterized by high resolution transmission electron microscope (HRTEM). Nanoparticles are well dispersed in non-polar solvent as toluene. The size of synthesized silver nanoparticles is up to 20 nm and the smallest size of silver nanoparticles is to 10 from 5 nm. It was shown that factors governing the size of silver nanoparticles are reaction time, temperature and concentration of solutes. These smallest silver nanoparticles can be effective to make silver colloid sinter under 200 oC. It can be high-loaded up to silver nanoparticle 80 wt.% with consequence that is measured by thermo gravimetric analyzer (TGA). |
| 저자 |
김윤성1, 이종택2, 윤호규3
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| 소속 |
1고려대, 2Corporate R&D, 3LG Chem. Research Park |
| 키워드 |
non-polar; silver nano particle; sintering temperature; high-loading
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| E-Mail |
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