| 학회 |
한국재료학회 |
| 학술대회 |
2014년 가을 (11/27 ~ 11/28, 대전컨벤션센터) |
| 권호 |
20권 2호 |
| 발표분야 |
C. 에너지/환경 재료(Energy and Environmental Materials) |
| 제목 |
Effects of the synthesis conditions to the formation of TiO2 nanotube by microwave-assisted hydrothermal method |
| 초록 |
TiO2 nanotubes (TNT) synthesized by microwave-assisted hydrothermal method have more attention due to their unique properties: High surface area, ion exchange ability, high yield and low cost. The synthesis conditions such as: precursor, hydrothermal temperature and duration, post treatment (acid washing and calcination), the concentration of alkaline solution, auxiliary methods (ultrasonication and microwave-assistance) play an important role. Therefore, in this work we studied and indicated the effects of hydrothermal temperature (100oC-150oC), hydrothermal time (1-4 hour) and the concentration of NaOH solution (4M-10M) to the formation and properties of products. Samples were characterized by X-ray diffraction (XRD), Raman spectroscopy (RS), Transmission electron microscopy (TEM), Brunauer-Emmett-Teller (BET) and UV-vis DRS spectroscopy. The photocatalytic activity was investigated by degradation of Methylene Blue (MB). |
| 저자 |
Huy Hao Nguyen1, Sung Hun Cho2, Soo Wohn Lee1
|
| 소속 |
1Research Center for Eco Multi-Functional Nanomaterials, 2Sun Moon Univ. |
| 키워드 |
TiO2; nanotube; microwave; hydrothermal method; photocatalyst
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| E-Mail |
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