화학공학소재연구정보센터
학회 한국재료학회
학술대회 2014년 가을 (11/27 ~ 11/28, 대전컨벤션센터)
권호 20권 2호
발표분야 B. 나노 재료(Nanomaterials)
제목 Interface analysis between vertically aligned carbon nanotubes and graphene
초록 Nano carbon materials such as fullerene (0D), carbon nanotubes (1D) and graphene (2D) have become one of the most studied nanomaterials due to its high electrical, thermal and mechanical properties. Recently, three-dimensional (3D) hybrid carbon materials such as combination of CNT-graphene were most interested research topic due to their advantages for such practical application as in transparent conductive films, supercapacitors, lithium ion batteries and solar cells. In theoretical studies predicted CNT and graphene junction has C-C covalent bonds and it can be improved their own properties. However, experiment studies was not known surely how to CNT and graphene were connected in the interface due to their special form was difficult to prepare the sample for the transmission electron microscope (TEM) analysis. For this reasons, we were synthesized the vertically aligned CNTs on graphene sheet and pre-treatment the hybrid film before the TEM sample preparation process by focuesd ion beam. This strategy of sample preparation technique was able to investigate the interfacial analysis of 3D CNT-graphene hybrid film by TEM. And also, energy dispersive spectroscopy (EDS) and electron energy loss spectroscopy (EELS) analysis were performed for study of growth mechanism and elemental distribution. These interfacial characterization results will be able to explain the 3D hybrid nano-carbon structure.
저자 이양진1, 곽봉원2, 이진선2, 이병수2, 황준연1
소속 1한국과학기술(연), 2전북대
키워드 Graphene; Carbon nanotube; Interface; Transmission electron microsocpy
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