| 학회 |
한국재료학회 |
| 학술대회 |
2006년 가을 (11/03 ~ 11/03, 수원대학교) |
| 권호 |
12권 2호 |
| 발표분야 |
나노 및 생체 재료 |
| 제목 |
Synthesis and Characterization of metallic Ir embedded SiO2 Nanoparticles by a Reverse Micelle and Sol-Gel Processing |
| 초록 |
Metallic Ir clusters were embedded into a SiO2 nanoparticles have been synthesized within reverse micelle via a solution reduction of Ir(NO3)2 by hydrazine hydrate. The size of the particles can be controlled by manipulating the relative rates of the hydrolysis and condensation reactions of TEOS within the micro-emulsion. The spherical equivalent size for the Ir clusters formed in SiO2 matrix is estimated to be around 31nm. The presence of Ir in the matrix was demonstrated by EDS spectroscopy. The effects of synthesis parameters, such as the concentration of Ir solution, the molar ratio of water to TEOS and the molar ratio of water to surfactant, are discussed. |
| 저자 |
Jeong Hun Son1, Dong-Sik Bae2
|
| 소속 |
11School of Nano & Advanced Materials Science Engineering, 2Changwon National Univ. |
| 키워드 |
Ir embedded SiO2; Nanoparticles; Reverse Micelle Process
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| E-Mail |
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