화학공학소재연구정보센터
학회 한국공업화학회
학술대회 2022년 봄 (05/11 ~ 05/13, 제주국제컨벤션센터(ICC JEJU))
권호 26권 1호
발표분야 [나노] 나노튜브를 중심으로 한 상용화 기술
제목 Purification and debundling of SWCNT via Supercritical Fluid Treatments
초록 Single-walled carbon nanotube (SWCNT) was treated with Carbon dioxide supercriticalfluids (CO2-SCF) containing surfactant solution. Compared to the untreatedone, SCF-treated SWCNT was easily dispersed in an aqueous surfactant solution withoutobvious damage by gentle ultrasonication. We found that lots of metal impurity wasremoved by the treatments confirmed by SEM, EDX and TGA analysis. Metallic andsemiconducting components of SWCNT were found to be effectively separated usinga gel chromatography. It noted that SWCNT are more debundled after the SCFtreatment. Metallic and semiconducting components were quantitatively analyzedusing Near-IR spectroscopy along with Raman spectroscopy.
저자 서영수
소속 세종대
키워드 SWCNT; Supercritical fluid; debundling; Dispersion
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