화학공학소재연구정보센터
학회 한국공업화학회
학술대회 2019년 봄 (05/01 ~ 05/03, 부산 벡스코(BEXCO))
권호 23권 1호
발표분야 석유화학·윤활유_포스터
제목 Mesophase Pitch from Petroleum Residue by a Non-Catalytic Method
초록 Pitch was synthesized from fluidized catalytic cracking decant oil as a raw material by a two-step heat treatment technique to investigate the mesophase content of the resulting pitch as a function of the synthetic temperature and time. Thermogravimetric and softening point (SP) analyses were performed to observe the thermal behaviors of the pitch. Structural properties were also analyzed by X-ray diffraction. Molecular weight distribution was determined by a matrix-assisted laser desorption/ionization time-of-flight mass spectrometry analysis. Chemical structures and the number of and aromatic components were examined by a nuclear magnetic resonance and a Fourier-transform infrared spectroscopy analysis. The anisotropy/isotropy of the pitch was also observed by a polarizing microscope. The SP and carbon yield gradually increased with increasing synthetic temperature and time. The anisotropic content varies depending on the heat treatment conditions.
저자 최용환, 이동훈, 김병주
소속 한국탄소융합기술원
키워드 Mesophase; Pitch; Petroleum residue; Heat treatment
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