Optimization of ionic liquid assisted sugar conversion and nanofiltration membrane separation for 5-hydroxymethylfurfural

Ariyanti Sarwono; Zakaria Man; Alamin Idris; Amir Sada Khan; Nawshad Muhammad; Cecilia Devi Wilfred

Journal of Industrial and Engineering Chemistry, Vol.69, 171-178, January, 2019

DOI10.1016/j.jiec.2018.09.020 Export Citation

Optimization of ionic liquid assisted sugar conversion and nanofiltration membrane separation for 5-hydroxymethylfurfural

Ariyanti Sarwono^{1, 2, †}, Zakaria Man¹, Alamin Idris¹, Amir Sada Khan³, Nawshad Muhammad⁴, and Cecilia Devi Wilfred¹

¹Centre of Research in Ionic Liquids(CORIL), Universiti Teknologi PETRONAS (UTP), 31750, Tronoh, Perak, Malaysia
²Department of Environmental Engineering, Pertamina University, Kebayoran Lama, 12220, Jakarta, Indonesia
³Department of Chemistry, University of Science and Technology, Bannu 28100, Khyber Pakhtunkhwa, Pakistan
⁴Interdisciplinary Research Centre in Biomedical materials, COMSATS Institute of Information Technology, Lahore, Pakistan

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This paper provides complete loop of ionic liquid (IL) assisted glucose conversion to 5-hydroxyme- thylfurfural (HMF), nanofiltration membrane (NF) based separation and recyclability. The optimum HMF yield of 65.6% was obtained with 8 wt.% catalyst loading at 125 °C reaction temperature in 120 min reaction time. Ea for conversion was found to be 120 kJ/mol. NF was adopted first time to separate IL and HMF. The percentage of recovered HMF using NF for 1st, 2nd and 3rd batches are 94.87, 84.35 and 71.65 respectively. The structures of regenerated IL and HMF, obtained from NF and liquid.liquid extraction, were confirmed by NMR.

Keywords:Ionic liquids;Nanofiltration membrane;Conversion;5-Hydroxymethylfurfural;Response surface methodology

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[Referenced By]

[1] Wang F, Yuan Z, Liu B, Chen S, Zhang Z, J. Ind. Eng. Chem., 38, 181 (2016)

[2] Catrinck MN, Ribeiro ES, Monteiro RS, Ribas RM, Barbosa MHP, Teofilo RF, Fuel, 210, 67 (2017)

[3] Swatloski RP, Spear SK, Holbrey JD, Rogers RD, J. Am. Chem. Soc., 124(18), 4974 (2002)

[4] Sarwono A, Man Z, Muhammad N, Khan AS, Hamzah WSW, Rahim AHA, Ullah Z, Wilfred CD, Ultrason. Sonochem., 37, 310 (2017)

[5] Khan AS, Man Z, Bustam MA, Nasrullah A, Ullah Z, Sarwono A, Shah FU, Muhammad N, Carbohydr. Polym., 181, 208 (2018)

[6] Ramli NAS, Amin NAS, J. Mol. Catal. A-Chem., 407, 113 (2015)

[7] Wu L, Song J, Zhang B, Zhou B, Zhou H, Fan H, Yang Y, Han B, Green Chem., 16, 3935 (2014)

[8] Tao F, Song H, Chou L, Carbohydr. Res., 346, 58 (2011)

[9] Tao FR, Zhuang C, Cui YZ, Xu J, Chin. Chem. Lett., 25, 757 (2014)

[10] Li H, Zhang QY, Liu XF, Chang F, Zhang YP, Xue W, Yang S, Bioresour. Technol., 144, 21 (2013)

[11] Qi X, Watanabe M, Aida TM, Smith RL, ChemSusChem, 3, 1071 (2010)

[12] Liu W, Zheng F, Li J, Cooper A, AIChE J., 60(1), 300 (2014)

[13] Garcia S, Larriba M, Garcia J, Torrecilla JS, Rodriguez F, J. Chem. Thermodyn., 45(1), 68 (2012)

[14] Toh SLI, McFarlane J, Tsouris C, DePaoli DW, Luo H, Dai S, Solvent Extr. Ion Exch., 24, 33 (2006)

[15] Abu-Eishah SI, Ionic Liquids - Classes and Properties, InTech, 2011.

[16] Han S, Wong HT, Livingston AG, Chem. Eng. Res. Des., 83(A3), 309 (2005)

[17] Hazarika S, Sci. Cult., 77, 503 (2011)

[18] Qi BK, Luo JQ, Chen GQ, Chen XR, Wan YH, Bioresour. Technol., 104, 466 (2012)

[19] Hou Q, Li W, Ju M, Liu L, Chen Y, Yang Q, RSC Adv., 6, 104016 (2016)

[20] Myers RH, Montgomery DC, Response Surface Methodology: Process and Product Optimization Using Designed Experiments, John Wiley & Sons, 1995.

[21] Sharif KM, Rahman MM, Azmir J, Shamsudin SH, Uddin MS, Fahim TK, Zaidul ISM, J. Ind. Eng. Chem., 21, 1314 (2015)

[22] Zhang Z, Wang Q, Xie H, Liu W, Zhao ZK, ChemSusChem, 4, 131 (2011)

[23] Ramli NAS, Amin NAS, Energy Conv. Manag., 95, 10 (2015)

[24] Zhao H, Holladay JE, Brown H, Zhang ZC, Science, 316, 1597 (2007)

[25] Nguyen CV, Lewis D, Chen WH, Huang HW, Al Othman ZA, Yamauchi Y, Wu KCW, Catal. Today, 278, 344 (2016)

[26] Rasrendra CB, Soetedjo JNM, Makertihartha IGBN, Adisasmito S, Heeres HJ, Top Catal., 55, 543 (2012)

[27] Hu L, Wu Z, Xu J, Sun Y, Lin L, Liu S, J. Chem. Eng., 244, 137 (2014)

[28] Zhang J, Cao Y, Li H, Ma X, J. Chem. Eng., 237, 55 (2014)